Combustion Synthesis of B4C–TiB2 Composite Nanoparticle by Self-Propagating High-Temperature Synthesis (SHS) in B2O3–TiO2–Mg–C System

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dc.authorscopusid57222375761
dc.authorscopusid55657674000
dc.authorscopusid57211354289
dc.authorscopusid57211514953
dc.contributor.authorCoban, O.
dc.contributor.authorBugdayci, M.
dc.contributor.authorBaslayici, S.
dc.contributor.authorAcma, M.E.
dc.date.accessioned2024-06-13T20:15:57Z
dc.date.available2024-06-13T20:15:57Z
dc.date.issued2023
dc.departmentİstanbul Gedik Üniversitesi
dc.descriptionAdvances in Powder and Ceramic Materials Science Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023 -- 19 March 2023 through 23 March 2023 -- -- 292179
dc.description.abstractIn this study, B4C-TiB2 nanocomposite powder was synthesized from oxide raw materials with the principle of magnesiothermic reduction in B2O3–TiO2–Mg–C system by SHS method. For the SHS process, Mg and C stoichiometries were optimized with thermochemical simulation, and composite charge stoichiometry and Mg particle size were optimized with XRD, BET and SEM analyzes. Optimization of acid concentration, leaching temperature, and leaching time parameters has been provided for the HCl leaching processes carried out to remove undesired by-products after SHS. In addition, pH and temperature changes during leaching were analyzed and an innovative application of modified leaching with H2O2 and carbonic acid addition was investigated. The results showed that by optimizing the process steps for the synthesis of B4C–TiB2 composite nanoparticle by the SHS method, a commercial grade product with a surface area of 30.6 m2/g, and a particle size of 193 nm was obtained. © 2023, The Minerals, Metals & Materials Society.
dc.identifier.doi10.1007/978-3-031-22622-9_16
dc.identifier.endpage169
dc.identifier.isbn9783031226212
dc.identifier.issn2367-1181
dc.identifier.scopus2-s2.0-85151136888
dc.identifier.scopusqualityQ3
dc.identifier.startpage161
dc.identifier.urihttps://doi.org/10.1007/978-3-031-22622-9_16
dc.identifier.urihttps://hdl.handle.net/11501/982
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer Science and Business Media Deutschland GmbH
dc.relation.ispartofMinerals, Metals and Materials Series
dc.relation.publicationcategoryKonferans Öğesi - Uluslararası - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectAdvanced ceramics
dc.subjectBoron carbide
dc.subjectComposite powder
dc.subjectNanoparticle synthesis
dc.subjectTitanium diboride
dc.subjectBoron carbide
dc.subjectCarbon dioxide
dc.subjectChlorine compounds
dc.subjectCombustion synthesis
dc.subjectComposite materials
dc.subjectLeaching
dc.subjectNanoparticles
dc.subjectParticle size
dc.subjectScalability
dc.subjectStoichiometry
dc.subjectAdvanced Ceramics
dc.subjectC-systems
dc.subjectComposite nanoparticles
dc.subjectComposite powders
dc.subjectNanocomposite powder
dc.subjectNanoparticle synthesis
dc.subjectParticles sizes
dc.subjectSelf propagating high temperature synthesis
dc.subjectSynthesis method
dc.subjectTitanium diboride
dc.subjectTitanium dioxide
dc.titleCombustion Synthesis of B4C–TiB2 Composite Nanoparticle by Self-Propagating High-Temperature Synthesis (SHS) in B2O3–TiO2–Mg–C System
dc.typeConference Object

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