An extensive study on the synthesis of iron based magnetic aluminium oxide nanocomposites by solution combustion method

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dc.authorwosidOZBEK, BELMA/D-2884-2019
dc.contributor.authorPehlivan, Merve
dc.contributor.authorSimsek, Sinem
dc.contributor.authorOzbek, Sunullah
dc.contributor.authorOzbek, Belma
dc.date.accessioned2024-06-13T20:18:02Z
dc.date.available2024-06-13T20:18:02Z
dc.date.issued2019
dc.departmentİstanbul Gedik Üniversitesien_US
dc.description.abstractIn the present study, it was aimed to investigate the synthesis of iron based magnetic aluminium oxide nanocomposites (IMANCs) by solution combustion (SC) method using various fuel types at various amounts. IMANCs were synthesized using aluminium nitrate and iron nitrate as oxidizers. Urea, glycine and sucrose were chosen as fuel types at various amounts, respectively, to examine their effects on size and morphology of nanocomposites synthesized. The chemical compositions, morphologies and thermal behaviors of IMANCs synthesized were compared with data obtained from characterization studies using X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDS), Thermogravimetric and Differential Thermal Analysis (TG/DTA), Fourier Transform Infrared Analysis (FT-IR), Surface Area and Porosity Analyzer. The characterization studies revealed that IMANCs were synthesized successfully by SC method with nanoscale properties. It was found that IMANCs synthesized using stoichiometric amount of glycine had porous and smaller particle size with higher surface area compared to other samples synthesized by urea and sucrose, respectively. There is no documentation found on glycine based synthesis of IMANCs by SC method in the literature so far. Additionally, this original paper is the first report on the synthesis of IMANCs by applying calcination and reduction processes following SC reaction using various fuel types at various amounts. It was resulted that the samples synthesized by SC method had smaller particle sizes compared to the samples which were synthesized by applying calcination and reduction processes following SC reaction using stoichiometric amount of urea, glycine and sucrose as fuel types, respectively. (C) 2019 Brazilian Metallurgical, Materials and Mining Association. Published by Elsevier Editora Ltda.en_US
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK) [315M495]en_US
dc.description.sponsorshipThe present study was carried at both laboratories of Yildiz Technical University, Chemical Engineering Department and Istanbul Gedik University, Metallurgy and Materials Engineering Department. Also, this research has been supported by the Scientific and Technological Research Council of Turkey (TUBITAK), Project No. 315M495. Sinem Simsek gratefully acknowledges the Scientific and Technological Research Council of Turkey (TUBITAK) for the scholarship.en_US
dc.identifier.doi10.1016/j.jmrt.2018.12.005
dc.identifier.endpage1760en_US
dc.identifier.issn2238-7854
dc.identifier.issn2214-0697
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-85060765571en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1746en_US
dc.identifier.urihttps://doi.org/10.1016/j.jmrt.2018.12.005
dc.identifier.urihttps://hdl.handle.net/11501/1182
dc.identifier.volume8en_US
dc.identifier.wosWOS:000469405800018en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofJournal of Materials Research and Technology-Jmr&Ten_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectIron Based Magnetic Aluminium Oxide Nanocompositesen_US
dc.subjectFuel Typesen_US
dc.subjectSolution Combustion Methoden_US
dc.subjectCalcinationen_US
dc.subjectReductionen_US
dc.subjectCharacterization Studiesen_US
dc.subjectSol-Gelen_US
dc.subjectGranular Filmsen_US
dc.subjectNanoparticlesen_US
dc.subjectFuelen_US
dc.subjectCompositesen_US
dc.subjectNanostructuresen_US
dc.subjectDecompositionen_US
dc.subjectTemperatureen_US
dc.subjectCatalystsen_US
dc.subjectRemovalen_US
dc.titleAn extensive study on the synthesis of iron based magnetic aluminium oxide nanocomposites by solution combustion methoden_US
dc.typeArticleen_US

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